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2-bromo-1-[4-[4-(2-bromoacetyl)phenyl]phenyl]ethanone_4072-67-7

2-bromo-1-[4-[4-(2-bromoacetyl)phenyl]phenyl]ethanone

  • CAS:

    4072-67-7

  • Synonym:

    2-bromo-1-[4-[4-(2-bromoacetyl)phenyl]phenyl]ethanone
    1,1-(1,1-Biphenyl)-4,4-diylbis(2-bromoethan-1-one)
    1,1'-(4,4'-Biphenyldiyl)bis(2-bromoethanone)

Details

Chemical Name:    2-bromo-1-[4-[4-(2-bromoacetyl)phenyl]phenyl]ethanone
CAS.NO:4072-67-7
Synonyms:1,1-(1,1-Biphenyl)-4,4-diylbis(2-bromoethan-1-one)
1,1'-(4,4'-Biphenyldiyl)bis(2-bromoethanone)

Molecular Formula: C16H12Br2O2
Molecular Weight:396.07300

Physical and Chemical Properties:
Density: 1.622g / cm3
Boiling point: 464.8ºC at 760 mmHg
Flash point: 121.3ºC
Refractive index: 1.625

Specification:
Appearance: White crystalline powder
Purity:≥98.0%
Identification:
A .H-NMR:Comply with the structure
B.LC-MS:Comply with the structure
C.The IR spectrum of sample should be identical with that ofreference standard
D.HPLC-ESI-MS
The retention time of the major peak in the chromatogram ofthe Assay preparation corresponds to that in the chromatogram of the Standard preparation, as obtained inthe Assay.
Crystallization:meets the requirements.
Loss on drying:≤0,5%
Heavy metals:≤10 ppm
Water:≤1.0%
Sulphated ash:≤0. 2%, determined on 1.0 g.
Relatedsubstances:
Unspecified impurities: for each impurity≤0.10%
Total Impurity≤1.0%
Purity:≥99.0%
Assay:99.0%~ 101.0% (anhydrous substance).

Packing:
 25kgs packaging Fiber drum outside and plastic bag inside,1-25kgs packaging aluminium bag outside and double plastic bag inside.
Storage:Store in a well-closed container away from moisture.
Application: It can be used to synthesize Daclatasvir which inhibits the HCV protein NS5A, and thus can be used as a drug candidate for the treatment of hepatitis C (HCV).Intermediates of Daclatasvir CAS:1009119-64-5


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Laboratory in Ningbo
Our company's R&D company, Ningbo Gino Chemical Co., Ltd. was established in December 2011. we have several fume hoods and kilogram laboratory, and have purchased 20L, 50L reactors and as a preliminary pilot manufacturing of the products. At the same time, We mobilized external resources to establish a pilot facility in Henan Zhumadian and Anhui Anqing, and cooperating with Shandong Zibo and Jiangsu Changzhou factories as a large production facility for our products.

Factory in Shanxi Province
At the end of 2017, We invested workshop in Xinjiang County Longzhou Chemical Co., Ltd., Xinjiang County Coal Mine Park, Yuncheng, Shanxi. The first phase of the reactors were 30* 2000L~5000L, The contract output value is 50 million annually, factory has passed the audit from public listed company domestic and abroad.

Factory in Shandong Province
The production base of liquid rectification chemical products located in Liaocheng, Shandong Province is the main outsourcing production base of our company. The products are sold to leading enterprises and listed companies in the carcass industry for many years. The production, quality and service are stable, delivery is timely, and some individual products are covering 90% of the market.

Factory in Henan Province
In year 2020, We invested workshop in Henan province, the workshop consists of 50*2000L~5000L reactors, The types of reactions that can be manufacturer there are: bromination, cyanidation, and conventional reactions.

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