Methoxyethene, also widely recognized as Vinyl Methyl Ether (VME) and identified by CAS number 107-25-5, is a fundamental chemical intermediate with significant industrial applications. Its unique structure and reactivity make it a valuable building block, but its volatile and flammable nature also necessitates a thorough understanding of its properties and safe handling procedures. This article provides a detailed overview of Methoxyethene, including its synthesis methods, key chemical and physical properties, and critical safety information for users in manufacturing and research environments.

Synthesis Routes for Methoxyethene

Industrially, Methoxyethene is primarily synthesized through two main pathways:

  • Acetylene and Methanol Route (Reppe Process): This method involves the reaction of acetylene with methanol in the presence of a strong base catalyst. While effective, this process often requires high temperatures and pressures, posing safety challenges due to the handling of acetylene gas. Optimized versions utilize catalysts like ZnO/SiO2 at moderate temperatures.
  • Dimethyl Acetal Pyrolysis: A more common and safer method involves the high-temperature pyrolysis of dimethyl acetal in the vapor phase, often over a solid catalyst like calcium phosphate. This process yields Methoxyethene and methanol, with high selectivity and conversion rates.

For procurement managers and R&D scientists, understanding the synthesis route can provide insights into potential impurities and the overall quality of the Methoxyethene they intend to purchase.

Key Chemical and Physical Properties

Methoxyethene (C3H6O, MW: 58.08) exhibits several key properties relevant to its industrial use:

  • Appearance: Colorless gas at room temperature, often supplied as a liquefied gas.
  • Melting Point: -122 °C
  • Boiling Point: 6 °C
  • Density: Approximately 0.7440 g/cm³
  • Solubility: Slightly soluble in water, but readily soluble in ethanol, ether, and acetone.
  • Reactivity: Highly flammable. Prone to polymerization, especially in the presence of acids or heat. Can form dangerous peroxides upon exposure to air. Reacts vigorously with oxidizing materials.

The propensity for polymerization and peroxide formation means that Methoxyethene is typically stored and transported with a polymerization inhibitor.

Safety Considerations for Handling Methoxyethene

Given its flammable nature and reactivity, strict safety protocols are essential when handling Methoxyethene:

  • Flammability: VME is extremely flammable. Sources of ignition, including sparks, open flames, and static discharge, must be avoided. Ensure adequate ventilation to prevent the buildup of flammable vapors.
  • Peroxide Formation: Like many ethers, Methoxyethene can form explosive peroxides. It should be stored in airtight containers away from light and air, and regularly tested for peroxides if stored for extended periods.
  • Polymerization Hazards: Contact with acids can trigger rapid, exothermic polymerization. Store away from acidic materials.
  • Health Hazards: Inhalation of high concentrations can cause intoxication, dizziness, and other central nervous system effects. Contact with the liquid can cause frostbite.

When you buy Methoxyethene, always consult the Safety Data Sheet (SDS) provided by the manufacturer for detailed handling and emergency procedures. NINGBO INNO PHARMCHEM CO.,LTD. partners with reputable Chinese manufacturers to ensure you receive Methoxyethene (CAS 107-25-5) that adheres to high safety and quality standards. Contact us to discuss your sourcing needs.